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Makarochkinite

A valid IMA mineral species

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Makarochkinite, etc.

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite, etc.

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite, etc.

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite, etc.

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite, etc.

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Makarochkinite

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

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About MakarochkiniteHide

Formula:

(Ca,Na)₄[Fe²⁺₈Fe³⁺₂Ti₂]O₄[Si₈Be₂Al₂O₃₆]

Colour:

black

Lustre:

Vitreous

Hardness:

5½ - 6

Specific Gravity:

3.93

Crystal System:

Triclinic

Member of:

Rhönite Group > Sapphirine Supergroup

Name:

Named in honor of Boris Alexandrovich Makarochkin (Борис Александрович Макарочкин) (1908-1988), Russian chemist and mineralogist who studied rare minerals of the Ilmen Mountains, who worked for many years in the Ilmensky Reserve.

Type Locality:

ⓘ Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Aenigmatite Group. Close related with Høgtuvaite.

Unique IdentifiersHide

Mindat ID:

2547

Long-form identifier:

mindat:1:1:2547:4

IMA Classification of MakarochkiniteHide

IMA status:

Approved

IMA Formula:

Ca₄[Fe²⁺₈Fe³⁺₂Ti⁴⁺₂]O₄[Si₈Be₂Al₂O₃₆]

Approval year:

2003

Classification of MakarochkiniteHide

Strunz-mindat (2026):

9.DH.40

9 : SILICATES (Germanates)
D : Inosilicates
H : Inosilicates with 4-periodic single chains, Si₄O₁₂

Mineral SymbolsHide

As of 2021 there are now IMA–CNMNC approved mineral symbols (abbreviations) for each mineral species, useful for tables and diagrams.

Symbol	Source	Reference for Standard
Mkr	IMA–CNMNC	Warr, L.N. (2021). IMA–CNMNC approved mineral symbols. Mineralogical Magazine, 85(3), 291-320. doi:10.1180/mgm.2021.43

Physical Properties of MakarochkiniteHide

Lustre:

Vitreous

Transparency:

Opaque

Colour:

Black

Hardness:

5½ - 6 on Mohs scale

Tenacity:

Brittle

Cleavage:

None Observed

Fracture:

Irregular/Uneven

Density:

3.93 g/cm³ (Measured) 3.933 g/cm³ (Calculated)

Optical Data of MakarochkiniteHide

Type:

Biaxial

RI values:

n_α = 1.821 - 1.849 n_γ = 1.85 - 1.88

Max. Birefringence:

δ = 0.029 - 0.031
Based on recorded range of RI values above.

Interference Colours:
The colours simulate birefringence patterns seen in thin section under crossed polars. They do not take into account mineral colouration or opacity.

Michel-Levy Bar The default colours simulate the birefringence range for a 30 µm thin-section thickness. Adjust the slider to simulate a different thickness.

Grain Simulation You can rotate the grain simulation to show how this range might look as you rotated a sample under crossed polars. Each grain retains its interference colour (retardation) while its brightness falls to black at extinction and reaches a maximum between extinction positions.

Thickness: 30 µm Order divisions

Rotation:

Surface Relief:

Very High (positive)
Relative to Canada balsam mounting medium (n ≈ 1.537).

This shows the grain boundary and Becke line effect under plane-polarised light, based on the contrast between this mineral's average refractive index and the mounting medium. It does not take into account mineral colouration.

Focus:

In focus

Pleochroism:

Visible

Comments:

X = greenish brown, Y = yellowish brown, Z = reddish brown; Y ≤ X < Z

Chemistry of MakarochkiniteHide

Mindat Formula:

(Ca,Na)₄[Fe²⁺₈Fe³⁺₂Ti₂]O₄[Si₈Be₂Al₂O₃₆]

Element Weights:

Element	% weight
O	36.546 %
Fe	31.891 %
Si	12.831 %
Ca	9.155 %
Ti	5.467 %
Al	3.082 %
Be	1.029 %

Calculated from ideal end-member formula.

Elements listed:

Al, Be, Ca, Fe, Na, O, Si, Ti - search for minerals with similar chemistry

Common Impurities:

Na,Mn,Mg

Crystallography of MakarochkiniteHide

Crystal System:

Triclinic

Class (H-M):

1 - Pedial

Space Group:

Cell Parameters:

a = 10.355 Å, b = 10.751 Å, c = 8.873 Å
α = 105.707°, β = 96.227°, γ = 124.861°

Ratio:

a:b:c = 0.963 : 1 : 0.825

Unit Cell V:

735.7 Å³

Twinning:

absent

Crystal StructureHide

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Unit Cell | Unit Cell Packed
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Data courtesy of the American Mineralogist Crystal Structure Database. Click on an AMCSD ID to view structure

ID	Species	Reference	Link	Year	Locality	Pressure (GPa)	Temp (K)
0014190	Makarochkinite	Yakubovich O V, Malinovskii Y A, Polyakov V O (1990) Crystal structure of makarochkinite of the Il'menskii National Forest, Russia Kristallografiya 35 1388-1394		1990	From type locality, a granite pegmatite in mine 400	0	293

CIF Raw Data - click here to close

data_global
_chemical_name_mineral 'Makarochkinite'
loop_
_publ_author_name
'Yakubovich O V'
'Malinovskii Y A'
'Polyakov V O'
_journal_name_full 'Kristallografiya'
_journal_volume 35 
_journal_year 1990
_journal_page_first 1388
_journal_page_last 1394
_publ_section_title
;
 Crystal structure of makarochkinite
 of the Il'menskii National Forest, Russia
;
_database_code_amcsd 0014190
_chemical_compound_source 'From type locality, a granite pegmatite in mine 400'
_chemical_formula_sum '(Ca3.5 Na.5) Fe10.3 Ti1.2 Mg.5 Si8.8 Be2 Al1.2 O40'
_cell_length_a 10.352
_cell_length_b 10.744
_cell_length_c 8.864
_cell_angle_alpha 105.73
_cell_angle_beta 96.16
_cell_angle_gamma 124.91
_cell_volume 733.912
_exptl_crystal_density_diffrn      3.924
_symmetry_space_group_name_H-M 'P -1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '-x,-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
Ca1   0.21707   0.63163   0.39356   0.90000   0.01279
Na1   0.21707   0.63163   0.39356   0.10000   0.01279
Ca2   0.65229   0.60165   0.37805   0.85000   0.01418
Na2   0.65229   0.60165   0.37805   0.15000   0.01418
Fe3+1   0.00000   0.00000   0.50000   0.80000   0.00887
Ti1   0.00000   0.00000   0.50000   0.10000   0.00887
Mg1   0.00000   0.00000   0.50000   0.10000   0.00887
Fe3+2   0.00000   0.50000   0.00000   0.90000   0.00887
Ti2   0.00000   0.50000   0.00000   0.10000   0.00887
Fe2+3   0.32197   0.85966   0.17432   0.95000   0.00861
Mg3   0.32197   0.85966   0.17432   0.05000   0.00861
Fe2+4   0.76900   0.82155   0.14411   0.95000   0.00975
Mg4   0.76900   0.82155   0.14411   0.05000   0.00975
Fe2+5   0.09463   0.94084   0.06155   0.90000   0.00874
Mg5   0.09463   0.94084   0.06155   0.10000   0.00874
Fe2+6   0.59473   0.94052   0.06206   1.00000   0.00925
Fe3+7   0.99571   0.73865   0.26034   0.50000   0.00912
Ti7   0.99571   0.73865   0.26034   0.50000   0.00912
Si1   0.46933   0.23668   0.33228   0.40000   0.00709
Be1   0.46933   0.23668   0.33228   0.50000   0.00709
Al1   0.46933   0.23668   0.33228   0.10000   0.00709
Si2   0.98333   0.23634   0.34350   0.80000   0.00747
Al2   0.98333   0.23634   0.34350   0.20000   0.00747
Si3   0.78613   0.34289   0.24134   0.70000   0.00646
Al3   0.78613   0.34289   0.24134   0.30000   0.00646
Si4   0.27318   0.33686   0.22679   0.50000   0.00697
Be4   0.27318   0.33686   0.22679   0.50000   0.00697
Si5   0.64411   0.94279   0.44510   1.00000   0.00697
Si6   0.35651   0.55814   0.05077   1.00000   0.00709
O1   0.34920   0.06540   0.16440   1.00000   0.01089
O2   0.85730   0.06580   0.17290   1.00000   0.01165
O3   0.55470   0.95540   0.29400   1.00000   0.01140
O4   0.01830   0.93480   0.26720   1.00000   0.01634
O5   0.24170   0.87490   0.39360   1.00000   0.01077
O6   0.75020   0.87850   0.38990   1.00000   0.01102
O7   0.49430   0.19600   0.49520   1.00000   0.01089
O8   0.95490   0.78000   0.48860   1.00000   0.01153
O9   0.89070   0.32000   0.37990   1.00000   0.01153
O10   0.39640   0.33820   0.36080   1.00000   0.01013
O11   0.65850   0.16980   0.06710   1.00000   0.01178
O12   0.14890   0.16460   0.06220   1.00000   0.01279
O13   0.52660   0.71010   0.03930   1.00000   0.01064
O14   0.06690   0.73480   0.06440   1.00000   0.01570
O15   0.24590   0.61270   0.11630   1.00000   0.01077
O16   0.74760   0.60200   0.13230   1.00000   0.01077
O17   0.39910   0.49730   0.18630   1.00000   0.01039
O18   0.94210   0.51390   0.22510   1.00000   0.01013
O19   0.16020   0.37180   0.31860   1.00000   0.01140
O20   0.66700   0.36970   0.33760   1.00000   0.01064

X-Ray Powder DiffractionHide

Powder Diffraction Data:

d-spacing	Intensity
7.997 Å	(57)
4.779 Å	(29)
3.120 Å	(32)
2.924 Å	(69)
2.676 Å	(77)
2.530 Å	(100)
2.410 Å	(28)
2.075 Å	(39)

Locality:

Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

Comments:

Format: d-spacing/Å (I) (hkl)

Geological EnvironmentHide

Paragenetic Mode(s):

Paragenetic Mode	Earliest Age (Ga)
Stage 5: Initiation of plate tectonics	<3.5-2.5
40 : Regional metamorphism (greenschist, amphibolite, granulite facies)

Type Occurrence of MakarochkiniteHide

Type Locality:

ⓘ Pit No. 400, Argayashsky District, Chelyabinsk Oblast, Russia

General Appearance of Type Material:

equant masses, 5-50 mm across

Geological Setting of Type Material:

granitic pegmatite

Associated Minerals at Type Locality:

Biotite	Columbite-(Fe)	Danalite	Fergusonite-(Y)	Ferro-edenite
Hastingsite	Ilmenite	Magnetite	Phenakite	Samarskite-(Y)
Titanite

Synonyms of MakarochkiniteHide

IMA2002-009a

Other Language Names for MakarochkiniteHide

Dutch:Makarochkiniet

German:Makarochkinit

Russian:Макарочкинит

Spanish:Makarochkinita

Relationship of Makarochkinite to other SpeciesHide

Member of:

Rhönite Group > Sapphirine Supergroup

Other Members of Rhönite Group:

Dorrite	Ca₄(Mg₃Fe³⁺₉)O₄(Si₃Al₈Fe³⁺O₃₆)	Tric.
Høgtuvaite	Ca₄[Fe²⁺₆Fe³⁺₆]O₄[Si₈Be₂Al₂O₃₆]	Tric. 1 : P1
Kuratite	Ca₂(Fe²⁺₅Ti)O₂[Si₄Al₂O₁₈]	Tric. 1 : P1
'Leucorhönite'	Ca₂(Mg,Fe³⁺,Al)₆(Si,Al)₆O₂₀	Tric.
Rhönite	Ca₄[Mg₈Fe³⁺₂Ti₂]O₄[Si₆Al₆O₃₆]	Tric. 1 : P1
Serendibite	Ca₄[Mg₆Al₆]O₄[Si₆B₃Al₃O₃₆]	Tric. 1 : P1
Welshite	Ca₄Mg₉Sb₃O₄[Si₆Be₃AlFe₂O₃₆]	Tric. 1 : P1

Common AssociatesHide

Associations Based on Photo Data:

5 photos of Makarochkinite associated with K Feldspar
4 photos of Makarochkinite associated with Quartz	SiO₂
1 photo of Makarochkinite associated with Titanite	CaTiO(SiO₄)

Related Minerals - Strunz-mindat Grouping Hide

9.DH.	Devilliersite	Ca₄Ca₂Fe³⁺₁₀O₄[(Fe³⁺₁₀Si₂)O₃₆]	Tric. 1 : P1
9.DH.	'Gageite-2M'	(Mn,Mg,Zn)₄₂Si₁₆O₅₄(OH)₄₀	Mon. 2/m
9.DH.	Bavsiite	Ba₂V₂O₂[Si₄O₁₂]	Tet. 4/m : I4/m
9.DH.	Yuzuxiangite	Sr₃Fe³⁺(Si₂O₆)₂(OH) · 3H₂O	Mon. 2/m : P2₁/m
9.DH.	Louisfuchsite	Ca₂(Mg₄Ti₂)(Al₄Si₂)O₂₀	Tric. 1 : P1
9.DH.05	Leucophanite	NaCaBeSi₂O₆F	Orth. 222 : P2₁2₁2₁
9.DH.10	Ohmilite	Sr₃(Ti,Fe³⁺)(Si₄O₁₂)(O,OH) · 2-3H₂O	Mon. 2/m : P2₁/m
9.DH.15	Haradaite	SrVSi₂O₇	Orth. mmm(2/m2/m2/m)
9.DH.15	Suzukiite	BaVSi₂O₇	Orth.
9.DH.20	Shcherbakovite	(K,Ba)KNa(Ti,Nb)₂(Si₄O₁₂)O₂	Orth. mmm(2/m2/m2/m) : Imma
9.DH.20	Batisite	BaNaNaTi₂(Si₄O₁₂)O₂	Orth. mmm(2/m2/m2/m) : Imma
9.DH.20	Noonkanbahite	BaKNaTi₂(Si₄O₁₂)O₂	Orth. mmm(2/m2/m2/m) : Imma
9.DH.25	Taikanite	Sr₃BaMn²⁺₂(Si₄O₁₂)O₂	Mon. 2 : B2
9.DH.30	Krauskopfite	BaSi₂O₅ · 3H₂O	Mon. 2/m : P2₁/b
9.DH.35	Gageite	Mn₂₁(Si₄O₁₂)₂O₃(OH)₂₀	Mon. 2/m
9.DH.35	Balangeroite	(Mg,Fe²⁺,Fe³⁺,Mn²⁺)₄₂Si₁₆O₅₄(OH)₄₀	Mon. 2/m
9.DH.40	Kuratite	Ca₂(Fe²⁺₅Ti)O₂[Si₄Al₂O₁₈]	Tric. 1 : P1
9.DH.40	Aenigmatite	Na₄[Fe²⁺₁₀Ti₂]O₄[Si₁₂O₃₆]	Tric. 1 : P1
9.DH.40	Dorrite	Ca₄(Mg₃Fe³⁺₉)O₄(Si₃Al₈Fe³⁺O₃₆)	Tric.
9.DH.40	Serendibite	Ca₄[Mg₆Al₆]O₄[Si₆B₃Al₃O₃₆]	Tric. 1 : P1
9.DH.40	Rhönite	Ca₄[Mg₈Fe³⁺₂Ti₂]O₄[Si₆Al₆O₃₆]	Tric. 1 : P1
9.DH.40	Khesinite	Ca₄(Mg₃Fe³⁺₉)O₄(Fe³⁺₉Si₃)O₃₆	Tric. 1 : P1
9.DH.40	'UM1991-29-SiO:FeMgNa'	Na₄(Mg₅Fe³⁺₇)O₄[Si₉Fe³⁺₃O₃₆]
9.DH.40	Høgtuvaite	Ca₄[Fe²⁺₆Fe³⁺₆]O₄[Si₈Be₂Al₂O₃₆]	Tric. 1 : P1
9.DH.40	'Leucorhönite'	Ca₂(Mg,Fe³⁺,Al)₆(Si,Al)₆O₂₀	Tric.
9.DH.40	Welshite	Ca₄Mg₉Sb₃O₄[Si₆Be₃AlFe₂O₃₆]	Tric. 1 : P1
9.DH.40	Wilkinsonite	Na₂Fe²⁺₄Fe³⁺₂(Si₆O₁₈)O₂	Tric. 1 : P1
9.DH.40	Krinovite	Na₂Mg₄Cr³⁺₂(Si₆O₁₈)O₂	Tric. 1 : P1
9.DH.45	Sapphirine	Mg₄(Mg₃Al₉)O₄[Si₃Al₉O₃₆]	Mon. 2/m : P2₁/b
9.DH.50	Khmaralite	(Mg,Al,Fe)₁₆[(Al,Si,Be)₁₂O₃₆]O₄	Mon. 2/m : P2₁/b
9.DH.55	'UM1988-26-SiO:AlMg'	Mg₄Al₂O[Si₃Al₂O₁₅]
9.DH.55	Surinamite	(Mg,Fe)₃Al₄BeSi₃O₁₆	Mon. 2/m
9.DH.60	Deerite	Fe²⁺₆Fe³⁺₃(Si₆O₁₇)O₃(OH)₅	Mon. 2/m : P2₁/b
9.DH.65	Taneyamalite	(Na,Ca)Mn²⁺₁₂(Si,Al)₁₂(O,OH)₄₄	Tric.
9.DH.65	Howieite	Na(Fe²⁺,Fe³⁺,Al,Mg)₁₂(Si₆O₁₇)₂(O,OH)₁₀	Tric. 1 : P1
9.DH.70	Johninnesite	Na₂Mn²⁺₉Mg₇(OH)₈[AsO₄]₂[Si₆O₁₇]₂	Tric.
9.DH.75	Agrellite	NaCa₂Si₄O₁₀F	Tric. 1 : P1

Other InformationHide

Health Risks:

No information on health risks for this material has been entered into the database. You should always treat mineral specimens with care.

Internet Links for MakarochkiniteHide

mindat.org URL:

https://www.mindat.org/min-2547.html
Please feel free to link to this page.

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Raman and XRD data at RRUFF project

References and PDF downloads at RRUFF project

American Mineralogist Crystal Structure Database

Mineral Dealers:

Buy from D. Joyce minerals

References for MakarochkiniteHide

Reference List:

Polyakov, V.O., Cherepivskaya, G.Ye. & Shcherbakova, Ye.P., (1986): Makarochkinite – a new beryllosilicate. In New and little-studied minerals and mineral associations of the Urals. Akad Nauk SSSR Ural’skiy Nauchnyy Tsentr. Sverdlovsk: 108–110. (in Russian)

Barbier, J., Britten, J., Grew, E. S., Hålenius, Ulf, Scherbakova, Y.P., Shearer, C.K., Yates, M. (2004) Makarochikinite, Ca2Fe2+4Fe3+TiSi4BeAlO20 - a new member of the aenigmatite group, and the Ti dominant analogue of høgtuvaite. GFF, 126 (1) 65-66 doi:10.1080/11035890401261sn8

Grew, E. S. (2005) Makarochkinite, Ca2Fe42+Fe3+TiSi4BeAlO20, a new beryllosilicate member of the aenigmatite-sapphirine-surinamite group from the Il'men Mountains (southern Urals), Russia. American Mineralogist, 90 (8) 1402-1412 doi:10.2138/am.2005.1759

Localities for MakarochkiniteHide

Showing 2 localities.

This map shows a selection of localities that have latitude and longitude coordinates recorded. Click on the

symbol to view information about a locality. The

symbol next to localities in the list can be used to jump to that position on the map.

Hide all sections | Show all sections

Locality ListHide

- This locality has map coordinates listed.

- This locality has estimated coordinates. ⓘ - Click for references and further information on this occurrence. ? - Indicates mineral may be doubtful at this locality.

- Good crystals or important locality for species.

- World class for species or very significant. (TL) - Type Locality for a valid mineral species. (FRL) - First Recorded Locality for everything else (eg varieties). ~~Struck out~~ - Mineral was erroneously reported from this locality. Faded * - Never found at this locality but inferred to have existed at some point in the past (e.g. from pseudomorphs).

All localities listed without proper references should be considered as questionable.


Russia (TL)
Chelyabinsk Oblast Argayashsky District ⓘ Pit No. 400 (TL)	Pekov (1998) +1 other reference
ⓘ Ilmen Nature Reserve	un2sg4.unige.ch (n.d.)

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Makarochkinite

About MakarochkiniteHide

Unique IdentifiersHide

IMA Classification of MakarochkiniteHide

Classification of MakarochkiniteHide

Mineral SymbolsHide

Physical Properties of MakarochkiniteHide

Optical Data of MakarochkiniteHide

Chemistry of MakarochkiniteHide

Crystallography of MakarochkiniteHide

Crystal StructureHide

X-Ray Powder DiffractionHide

Geological EnvironmentHide

Type Occurrence of MakarochkiniteHide

Synonyms of MakarochkiniteHide

Other Language Names for MakarochkiniteHide

Relationship of Makarochkinite to other SpeciesHide

Common AssociatesHide

Related Minerals - Strunz-mindat GroupingHide

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